Characterization of Solid Materials and Heterogeneous Catalysts
From Structure to Surface Reactivity
(Sprache: Englisch)
This two-volume book provides an overview of physical techniques used to characterize the structure of solid materials, on the one hand,
and to investigate the reactivity of their surface, on the other. Therefore this book is a must-have for anyone working...
and to investigate the reactivity of their surface, on the other. Therefore this book is a must-have for anyone working...
Leider schon ausverkauft
versandkostenfrei
Buch (Gebunden)
410.20 €
- Lastschrift, Kreditkarte, Paypal, Rechnung
- Kostenlose Rücksendung
- Ratenzahlung möglich
Produktdetails
Produktinformationen zu „Characterization of Solid Materials and Heterogeneous Catalysts “
This two-volume book provides an overview of physical techniques used to characterize the structure of solid materials, on the one hand,
and to investigate the reactivity of their surface, on the other. Therefore this book is a must-have for anyone working in fields related to surface
reactivity.
and to investigate the reactivity of their surface, on the other. Therefore this book is a must-have for anyone working in fields related to surface
reactivity.
Klappentext zu „Characterization of Solid Materials and Heterogeneous Catalysts “
This two-volume book provides an overview of physical techniques used to characterize the structure of solid materials, on the one hand,and to investigate the reactivity of their surface, on the other. Therefore this book is a must-have for anyone working in fields related to surface
reactivity. Among the latter, and because of its most important industrial impact, catalysis has been used as the directing thread of the book.
After the preface and a general introduction to physical techniques by M. Che and J.C. Védrine, two overviews on physical techniques are
presented by G. Ertl and Sir J.M. Thomas for investigating model catalysts and porous catalysts, respectively.
The book is organized into four parts: Molecular/Local Spectroscopies, Macroscopic Techniques, Characterization of the Fluid Phase (Gas and/
or Liquid), and Advanced Characterization. Each chapter focuses upon the following important themes: overview of the technique, most important parameters to interpret the experimental data, practical details, applications of the technique, particularly during chemical processes,
with its advantages and disadvantages, conclusions.
Inhaltsverzeichnis zu „Characterization of Solid Materials and Heterogeneous Catalysts “
PREFACE GENERAL INTRODUCTION
OVERVIEW ON PHYSICAL TECHNIQUES FOR INVESTIGATING MODEL SOLID CATALYSTS
OVERVIEW ON PHYSICAL TECHNIQUES FOR INVESTIGATING POROUS CATALYSTS LV
VOLUME 1
PART ONE MOLECULAR/LOCAL SPECTROSCOPIES
INFRARED SPECTROSCOPY
Introduction
Principles of IR Spectroscopy and Basic Knowledge for Its Use
Experimental Considerations
Use of IR Spectroscopy to Characterize Solids
Application to Surface Reactivity: Operando Spectroscopy
Conclusion
RAMAN AND UV-RAMAN SPECTROSCOPIES
Introduction
Characterization of Active Sites and Phase Structure of Metal Oxides
Characterization of Surface Metal Oxide Species on Supported Metal Oxides
Electron-Phonon Coupling in Nanostructured Materials
Characterization of sp2 Carbon Materials
Characterization of Transition Metal-Containing Microporous and Mesoporous Materials
Synthesis Mechanisms of Molecular Sieves
Conclusions
ELECTRONIC SPECTROSCOPY: ULTRA VIOLET-VISIBLE AND NEAR IR SPECTROSCOPIES
Introduction and Overview
UV-vis-NIR Spectra
Experimental Considerations
Formation and Alteration of Solids
Surface Reactivity and Catalysis
Conclusions
PHOTOLUMINESCENCE SPECTROSCOPY
Introduction
Basic Principles of Photoluminescence
General Aspects of Photoluminescence Measurements Characterization of Catalysts by Photoluminescence and Time-Resolved Photoluminescence Spectroscopy
Investigations of the Dynamics of Photocatalysis by Time-Resolved Photoluminescence Spectroscopy
Conclusion
NEUTRON SCATTERING
Introduction
Introduction to the Theory
Experimental
Structure
Dynamics
Conclusion
SUM FREQUENCY GENERATION AND INFRARED REFLECTION ABSORPTION SPECTROSCOPY
Introduction
Theoretical Background of SFG
Spectrometer Setup
Case Studies
Conclusion
INFRA RED REFLECTION ABSORPTION SPECTROSCOPY AND POLARISATION MODULATION-IRRAS
Introduction
Principle of IRAS
Principle of PM-IRAS
... mehr
Applications of IRAS and PM-IRAS
Conclusion
NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY
Introduction and Historical Perspective
Theory
Popular NMR Techniques for Studying Solids
Characterization of Heterogeneous Catalysts
Porosity, Adsorption, and Transport Processes
"In Situ" NMR
Towards "Operando" Studies
Conclusion and Outlook
ELECTRON PARAMAGNETIC RESONANCE SPECTROSCOPY
Introduction
Principles of EPR
Electron-Nucleus Hyperfine Interaction
Experimental Background
Anisotropy of Magnetic Interactions in EPR: the g, A, and D Tensors
EPR Spectra and the Solid State: Single Crystal Versus Powders
Guidelines to Interpretation of EPR Spectra
Computer Simulation of Powder Spectra
Molecular Interpretation of Parameters
Quantum Chemical Calculations of Magnetic Parameters
Advanced EPR Techniques
Characteristics of EPR Techniques in Application to Catalysis and Surfaces
Interfacial and Surface Charge-Transfer Processes
In Situ and Operando EPR Techniques
Conclusions and Prospects
MÖSSBAUER SPECTROSCOPY
Introduction
The Mössbauer Effect
Radiation Source
Mössbauer Absorbers
Hyperfine Interactions
Experimental Setups
Evaluation of Experimental Data
Theoretical Calculation of Mössbauer Parameters
Common Mössbauer-Active Transitions
Survey of Applications of the Mössbauer Effect in the Study of Catalytic Materials
Conclusion
LOW ENERGY ION SCATTERING AND SECONDARY ION MASS SPECTROMETRY
Introduction
Secondary Ion Mass Spectrometry
Low-Energy Ion Scattering (Ion Scattering Spectroscopy)
Single-Crystal and Polycrystalline Metal Surfaces
Amorphous Metallic Alloys
From Model to Real Catalysts
Conclusion
X-RAY ABSORPTION SPECTROSCOPY
In
Applications of IRAS and PM-IRAS
Conclusion
NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY
Introduction and Historical Perspective
Theory
Popular NMR Techniques for Studying Solids
Characterization of Heterogeneous Catalysts
Porosity, Adsorption, and Transport Processes
"In Situ" NMR
Towards "Operando" Studies
Conclusion and Outlook
ELECTRON PARAMAGNETIC RESONANCE SPECTROSCOPY
Introduction
Principles of EPR
Electron-Nucleus Hyperfine Interaction
Experimental Background
Anisotropy of Magnetic Interactions in EPR: the g, A, and D Tensors
EPR Spectra and the Solid State: Single Crystal Versus Powders
Guidelines to Interpretation of EPR Spectra
Computer Simulation of Powder Spectra
Molecular Interpretation of Parameters
Quantum Chemical Calculations of Magnetic Parameters
Advanced EPR Techniques
Characteristics of EPR Techniques in Application to Catalysis and Surfaces
Interfacial and Surface Charge-Transfer Processes
In Situ and Operando EPR Techniques
Conclusions and Prospects
MÖSSBAUER SPECTROSCOPY
Introduction
The Mössbauer Effect
Radiation Source
Mössbauer Absorbers
Hyperfine Interactions
Experimental Setups
Evaluation of Experimental Data
Theoretical Calculation of Mössbauer Parameters
Common Mössbauer-Active Transitions
Survey of Applications of the Mössbauer Effect in the Study of Catalytic Materials
Conclusion
LOW ENERGY ION SCATTERING AND SECONDARY ION MASS SPECTROMETRY
Introduction
Secondary Ion Mass Spectrometry
Low-Energy Ion Scattering (Ion Scattering Spectroscopy)
Single-Crystal and Polycrystalline Metal Surfaces
Amorphous Metallic Alloys
From Model to Real Catalysts
Conclusion
X-RAY ABSORPTION SPECTROSCOPY
In
... weniger
Autoren-Porträt
Michel Che completed his doctorate in 1968 at the University of Lyon and studied as postdoc at Princeton University (1969-1971). He was appointed Professor at University of Paris in 1975 and Senior Member of the Institut Universitaire de France in 1995. His work has led to around 400 publications in international journals. He has been very active in the promotion and organisation of catalysis, being the President-Founder of the European Federation of Catalysis Societies with creation in 1993 of the cycle of the now famous biennial "EuropaCat" congresses, and President of the International Association of Catalysis Societies in 2000-2004. His research activity has been largely devoted to catalytic processes, and he has pioneered a molecular approach to heterogeneous catalysis, based on transition elements taken as probes, specific isotopes and physical techniques, which endows him with an original position in the field. His work has led to the emergence of interfacial coordination chemistry at the junction of colloidal, electro-, supramolecular, geo- and solid-state chemistries. His studies have largely contributed to improve our understanding of the elementary processes involved in laboratory/industrial catalysis. Michel Che awards include J. H. Van't Hoff (Netherlands), Japan Society for the Promotion of Science (Japan), M. Sklodowska-Curie and P. Curie (Poland), A. Joannides and P. Sue (France), Von Humboldt - Gay-Lussac (Germany) and Centenary Price winner 2008 of the RSC (UK). He is Doctor honoris causa of several universities (Cracow, Poland; Lisbon, Portugal; Bucharest, Romania) and member of several high ranking academies (e.g. Academia Europaea, Deutsche Akademie der Naturforscher Leopoldina).Jacques C. V#;drine received a chemical engineering degree in 1962 from the Ecole Supérieure de Chimie Industrielle de Lyon, and his PhD in 1968 from the University of Lyon. Following several years of Postdoctoral research in the U.S., he returned to Lyon at the
... mehr
Institut de Recherches sur la Catalyse (IRC) as a Chargé de Recherche. In 1978 he was appointed head of the group working on metallic oxides (heterogeneous acid-type and partial oxidation catalysis fields) at IRC, in 1988 he became deputy director. In 1998 he moved to the University of Liverpool in the UK as Professor of Chemistry and Deputy Director of the Leverhulme Centre for Innovative Catalysis (LCIC) and Director of the European Associated Laboratory High Specificity Catalysis between CNRS and the University of Liverpool (LCIC-IRC). He returned to France in 2003 to join the Laboratoire de physico-chimie des surfaces de l'Ecole Nationale Supérieure de Chimie de Paris. He was also part time chargé de mission at the Ministry of National Education and Research. In 2006, he moved to the Laboratoire de Réactivité de Surface de l'Université de Paris VI. He was awarded the Grand prix Pierre SUE de la Société Française de Chimie in 2001. He was elected président de la Division de Catalyse de la Société Française de Chimie (1994-1997) and president of the European Federation of Catalysis Society for 1997-99.
He authored more than 450 publications in international journals and 7 books. His scientific interests cover heterogeneous catalysis (selective oxidation on mixed oxides and polyoxometallates and acid catalysis on zeolites, polyoxometallates, sulfated oxides, etc), combinatorial catalysis and physical techniques of catalyst characterisation.ry High Specificity Catalysis between CNRS and the University of Liverpool (LCIC-IRC). He returned to France in 2003 to join the Laboratoire de physico-chimie des surfaces de l'Ecole Nationale Supérieure de Chimie de Paris. He was also part time chargé de mission at the Ministry of National Education and Research. In 2006, he moved to the Laboratoire de Réactivité de Surface de l'Université de Paris VI. He was awarded the Grand prix Pierre SUE de la Société Française de Chimie in 2001. He was elected président de la Division de Catalyse de la Société Française de Chimie (1994-1997) and president
He authored more than 450 publications in international journals and 7 books. His scientific interests cover heterogeneous catalysis (selective oxidation on mixed oxides and polyoxometallates and acid catalysis on zeolites, polyoxometallates, sulfated oxides, etc), combinatorial catalysis and physical techniques of catalyst characterisation.ry High Specificity Catalysis between CNRS and the University of Liverpool (LCIC-IRC). He returned to France in 2003 to join the Laboratoire de physico-chimie des surfaces de l'Ecole Nationale Supérieure de Chimie de Paris. He was also part time chargé de mission at the Ministry of National Education and Research. In 2006, he moved to the Laboratoire de Réactivité de Surface de l'Université de Paris VI. He was awarded the Grand prix Pierre SUE de la Société Française de Chimie in 2001. He was elected président de la Division de Catalyse de la Société Française de Chimie (1994-1997) and president
... weniger
Bibliographische Angaben
- 2012, 1. Auflage, CII, 1182 Seiten, 116 farbige Abbildungen, 482 Schwarz-Weiß-Abbildungen, Maße: 17,8 x 25 cm, Gebunden, Englisch
- Herausgegeben: Michel Che, Jacques C. Vedrine
- Verlag: Wiley-VCH
- ISBN-10: 3527326871
- ISBN-13: 9783527326877
- Erscheinungsdatum: 12.04.2012
Sprache:
Englisch
Kommentar zu "Characterization of Solid Materials and Heterogeneous Catalysts"
Schreiben Sie einen Kommentar zu "Characterization of Solid Materials and Heterogeneous Catalysts".
Kommentar verfassen