Flash Chemistry (PDF)
Fast Organic Synthesis in Microsystems
(Sprache: Englisch)
Have you ever wished you could speed up your organic syntheses
without losing control of the reaction? Flash Chemistry is a
new concept which offers an integrated scheme for fast, controlled
organic synthesis. It brings together the generation of...
without losing control of the reaction? Flash Chemistry is a
new concept which offers an integrated scheme for fast, controlled
organic synthesis. It brings together the generation of...
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Have you ever wished you could speed up your organic syntheses
without losing control of the reaction? Flash Chemistry is a
new concept which offers an integrated scheme for fast, controlled
organic synthesis. It brings together the generation of highly
reactive species and their reactions in Microsystems to enable
highly controlled organic syntheses on a preparative scale in
timescales of a few seconds or less.
Flash Chemistry: Fast Organic Synthesis in microsystems is the
first book to describe this exciting new technique, with chapters
covering:
* an introduction to flash chemistry
* reaction dynamics: how fast is the act of chemical
transformation, what is the rate of reaction, and what determines
the selectivity of a reaction?
* examples of why flash chemistry is needed: the rapid
construction of chemical libraries, rapid synthesis of radioactive
PET probes, and on-demand rapid synthesis in industry
* the generation of highly reactive species through thermal,
microwave, chemical, photochemical, and electrochemical
activation
* microsystems: What are microsystems and how are they made? Why
is size so important? What are the characteristic features of
microsystems?
* conduction and control of extremely fast reactions using
microsystems
* applications of flash chemistry in organic synthesis
* polymer synthesis based on flash chemistry
* industrial applications of flash chemistry
Flash Chemistry: Fast Organic Synthesis in Microsystems is an
essential introduction to anyone working in organic synthesis,
process chemistry, chemical engineering and physical organic
chemistry concerned with fundamental aspects of chemical reactions
an d synthesis and the production of organic compounds.
without losing control of the reaction? Flash Chemistry is a
new concept which offers an integrated scheme for fast, controlled
organic synthesis. It brings together the generation of highly
reactive species and their reactions in Microsystems to enable
highly controlled organic syntheses on a preparative scale in
timescales of a few seconds or less.
Flash Chemistry: Fast Organic Synthesis in microsystems is the
first book to describe this exciting new technique, with chapters
covering:
* an introduction to flash chemistry
* reaction dynamics: how fast is the act of chemical
transformation, what is the rate of reaction, and what determines
the selectivity of a reaction?
* examples of why flash chemistry is needed: the rapid
construction of chemical libraries, rapid synthesis of radioactive
PET probes, and on-demand rapid synthesis in industry
* the generation of highly reactive species through thermal,
microwave, chemical, photochemical, and electrochemical
activation
* microsystems: What are microsystems and how are they made? Why
is size so important? What are the characteristic features of
microsystems?
* conduction and control of extremely fast reactions using
microsystems
* applications of flash chemistry in organic synthesis
* polymer synthesis based on flash chemistry
* industrial applications of flash chemistry
Flash Chemistry: Fast Organic Synthesis in Microsystems is an
essential introduction to anyone working in organic synthesis,
process chemistry, chemical engineering and physical organic
chemistry concerned with fundamental aspects of chemical reactions
an d synthesis and the production of organic compounds.
Inhaltsverzeichnis zu „Flash Chemistry (PDF)“
Preface. 1. Introduction. 1.1 Flask Chemistry. 1.2 Flash Chemistry. 1.3 Flask Chemistry or Flash Chemistry. 2. The Background to Flash Chemistry. 2.1 How do Chemical Reactions Take Place? 3. What is Flash Chemistry? 4. Why is Flash Chemistry Needed? 4.1 Chemical Reaction, an Extremely Fast Process at Molecular Level. 4.2 Rapid Construction of Chemical Libraries. 4.3 Rapid Synthesis of Radioactive Position Emission Tomography Probes. 4.4 On-Demand Rapid Synthesis in Industry. 4.5 Conclusions. 5. Methods of Activating Molecules. 5.1 Thermal Activation of Organic Molecules. 5.2 Photochemical Activation. 5.3 Electrochemical Activation. 5.4 Chemical Activation. 5.5 Accumulation of Reactive Species. 5.6 Continuous Generation of Reactive Species in a Flow System. 5.7 Interconversion Between Reactive Species. 5.8 Conclusions. 6. Control of Extremely Fast Reactions. 6.1 Mixing. 6.2 Temperature Control. 6.3 Residence Time Control. 6.4 Conclusions. 7. Microfluidic Devices and Microflow Systems. 7.1 Brief History. 7.2 Characteristic Features of Microflow Systems. 7.3 Microstructured Fluidic Devices. 7.4 Conclusions. 8. Applications of Flash Chemistry in Organic Synthesis. 8.1 Highly Exothermic Reactions that are Difficult to Control in Macrobatch Reactors. 8.2 Reactions in Which a Reactive Intermediate Easily Decomposes in Macrobatch Reactors. 8.3 Reactions with Products of Which Easily Decompose in Macrobatch Reactors. 8.4 Reactions in Which Undesired By-products are Produced in the Subsequent Reactions In Macrobatch Reactors. 8.5 Reactions That Can Be Accelerated Using Microflow Systems. 8.6 Conclusions. 9. Polymer Synthesis Based on Flash Chemistry. 9.1 Introduction. 9.2 Chain-Growth Polymerization and Step-Growth Polymerization. 9.3 Molecular Weight and Molecular-Weight Distribution. 9.4 Cationic Polymerization. 9.5 Free-Radical Polymerization. 9.6 Conclusions. 10. Industrial Applications of Flash Chemistry. 10.1 Synthesis of Diarylethene as Photochromic Compound
... mehr
(Micrometer-Size Single-Channel Reactor). 10.2 Synthesis of Pharmaceutically Interesting Spiro Lactone Fragment Of Nueropeptide Y (Millimeter-Size Channel-Single Reactor). 10.3 Grignard Exchange Process (Internal numbering-up). 10.4 Radical Polymerization Process (Numbering-up). 10.5 Other examples of Industrial Applications of Flash Chemistry . 10.6 Flash Chemistry as a Powerful Means of Sustainable Chemical Synthesis. 10.7 Conclusions. 11. Outlook of Flash Chemistry. Index.
... weniger
Autoren-Porträt von Jun-Ichi Yoshida
Professor Yoshida is head of the synthetic organic chemistry group at Kyoto University Graduate School of Engineering. His research activities concentrate on the development of methods to control and direct organic reactions.
Bibliographische Angaben
- Autor: Jun-Ichi Yoshida
- 2008, 1. Auflage, 244 Seiten, Englisch
- Verlag: John Wiley & Sons
- ISBN-10: 0470723416
- ISBN-13: 9780470723418
- Erscheinungsdatum: 13.10.2008
Abhängig von Bildschirmgröße und eingestellter Schriftgröße kann die Seitenzahl auf Ihrem Lesegerät variieren.
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