Multidimensional NMR Methods for the Solution State (PDF)

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The literature of multidimensional NMR began with the
publication of three papers in 1975, then nine in 1976 and fifteen
in 1977, and now contains many tens of thousands of papers. Any
attempt to survey the field must therefore necessarily be very
selective, not to say partial. In assembling this handbook, the
Editors have sought to provide both the new researcher and the
established scientist with a solid foundation for the understanding
of multidimensional NMR, a representative if inevitably limited
survey of its applications, an authoritative account of classic
techniques such as COSY, NOESY and TOSCY, and an account of the
latest progress in the development of multidimensional
techniques.

This handbook is structured in four parts. The first opens with
an historical introduction to, and a brief account of, the
practicalities and applications of multidimensional NMR methods,
followed by a definitive survey of their conceptual basis and a
series of articles setting out the generic principles of methods
for acquiring and processing multidimensional NMR data. In the
second part, the main families of multidimensional techniques,
arranged in approximate order of increasing complexity, are
described in detail, from simple J-resolved spectroscopy through to
the powerful heteronuclear 3D and 4D methods that now dominate the
study of structural biology in solution. The third part offers and
illustrative selection from the very wide range of applications of
multidimensional NMR methods, including some of the most recent
developments in protein NMR. Finally, the fourth part introduces
the idea of multidimensional spectra containing non-frequency
dimensions, in which properties such as diffusion and relaxation
are correlated.

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